Diastereoselective synthesis of half-sandwich chiral-at-metal cobaltacycles by oxidative cyclisation

Jahangir Amin; Christopher J. Richards

doi:10.1039/C2CC34837C

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Chemical Communications

Issue 82, 2012

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Diastereoselective synthesis of half-sandwich chiral-at-metal cobaltacycles by oxidative cyclisation

Jahangir Amin^a and Christopher J. Richards*^a

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School of Chemistry, University of East Anglia, Norwich Research Park, Norwich, UK
E-mail: Chris.Richards@uea.ac.uk ;
Fax: +44 (0)1603 592003 ;
Tel: +44 (0)1603 592003

Chem. Commun., 2012,48, 10192-10194

DOI: 10.1039/C2CC34837C
Received 06 Jul 2012, Accepted 09 Aug 2012
First published online 10 Aug 2012

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Reaction of chiral ester linked diynes with chlorotris(triphenylphosphine)cobalt(I) and sodium cyclopentadienide gave (η⁵-cyclopentadienyl)(triphenylphosphine) cobaltacyclopentadiene complexes as single chiral-at-metal diastereoisomers, including a non-racemic example synthesised in three steps from (S)-3-butyn-2-ol.

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Diastereoselective synthesis of half-sandwich chiral-at-metal cobaltacycles by oxidative cyclisation

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