The all-syn isomer of 1,2,4,5-tetrafluorocyclohexane is prepared and characterised by NMR and X-ray crystallography. It emerges to be a particularly polar cyclohexane analogue with differentially polarised faces.
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Fluorocyclohexanes: synthesis and structure of all-syn-1,2,4,5-tetrafluorocyclohexane
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a
University of St Andrews, School of Chemistry and Centre for Biomolecular Sciences, North Haugh, St Andrews, Fife, UK
E-mail: do1@st-andrews.ac.uk ;
Fax: +44 (0)1334 463800 ;
Tel: +44 (0)1334 467171
E-mail: do1@st-andrews.ac.uk ;
Fax: +44 (0)1334 463800 ;
Tel: +44 (0)1334 467171
b
Merck KGaA, Frankfurter Str. 250, D 64293 Darmstadt, Germany
Chem. Commun., 2012,48, 9643-9645
DOI: 10.1039/C2CC34679F
Received 29 Jun 2012, Accepted 03 Aug 2012
First published online 06 Aug 2012
Chemical Communications
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