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Reactions of 10-benzo[h]quinolyllithium with a series of organosilanes led to the formation of neutral pentacoordinate complexes. The diethynyl-substituted complex was able to be converted to di(arylethynyl)-substituted ones by the Sonogashira–Hagihara coupling reaction. Electronegative substituents shortened N–Si distances and enhanced fluorescence intensity from the complexes.
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