Highly enantioselective asymmetric hydrogenation of (E)-β,β-disubstituted α,β-unsaturated Weinreb amides catalyzed by Ir(I) complexes of SpinPhox ligands

Jian Shang; Zhaobin Han; Yang Li; Zheng Wang; Kuiling Ding

doi:10.1039/C2CC30812F

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Chemical Communications

Issue 42, 2012

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Highly enantioselective asymmetric hydrogenation of (E)-β,β-disubstituted α,β-unsaturated Weinreb amides catalyzed by Ir(I) complexes of SpinPhox ligands

Jian Shang,^a Zhaobin Han,^a Yang Li,^a Zheng Wang^a and Kuiling Ding*^a

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State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 345 Lingling Road, Shanghai, P.R. China
E-mail: kding@mail.sioc.ac.cn ;
Fax: +86 21 64166128

Chem. Commun., 2012,48, 5172-5174

DOI: 10.1039/C2CC30812F
Received 04 Feb 2012, Accepted 02 Apr 2012
First published online 03 Apr 2012

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The Ir(I) complexes of chiral spiro phosphino–oxazoline ligands (SpinPhox) have demonstrated good to excellent enantioselectivity in the asymmetric hydrogenation (AH) of a variety of (E)-β,β-disubstituted α,β-unsaturated N-methoxy-N-methylamides, affording the corresponding optically active Weinreb amides with up to 97% ee.

Abstract from Catalysts & Catalysed Reactions 2012

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Jian Shang
Zhaobin Han
Yang Li
Zheng Wang
Kuiling Ding

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Chemical Communications

Highly enantioselective asymmetric hydrogenation of (E)-β,β-disubstituted α,β-unsaturated Weinreb amides catalyzed by Ir(I) complexes of SpinPhox ligands

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Chemical Communications

Highly enantioselective asymmetric hydrogenation of (E)-β,β-disubstituted α,β-unsaturated Weinreb amides catalyzed by Ir(I) complexes of SpinPhox ligands

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