A modified sol–gel synthesis for non-oxide sulfide ceramics is presented. Sols are electrospun into continuous nanofiber precursors and then heat treated to obtain Chevrel-phase sulfide materials. In particular, the Mg-Chevrel fibers formed have average diameters of 230 ± 57 nm with grain sizes of 10 ± 3 nm after heat-treatment.
K. V. Woan, R. H. Scheffler, N. S. Bell and W. M. Sigmund, J. Mater. Chem., 2011, 21, 8537 DOI: 10.1039/C1JM10378D
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