An interlaboratory study of arsenic speciation analysis of whole blood

Kanna Ito; Walter Goessler; Hakan Gürleyük; Brian Wels; Christopher D. Palmer; Mary Frances Verostek; Patrick J. Parsons

doi:10.1039/C1JA10040H

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Journal of Analytical Atomic Spectrometry

Issue 9, 2011

Innovative research on the fundamental theory and application of spectrometric techniques.

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An interlaboratory study of arsenic speciation analysis of whole blood

Kanna Ito,^a^b Walter Goessler,^c Hakan Gürleyük,^d Brian Wels,^e Christopher D. Palmer,^a^b Mary Frances Verostek^a and Patrick J. Parsons*^a^b

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Laboratory of Inorganic and Nuclear Chemistry, Wadsworth Center, New York State Department of Health, P.O. Box 509, Albany, USA
E-mail: pparsons@wadsworth.org

Department of Environmental Health Sciences, School of Public Health, The University at Albany, P.O. Box 509, Albany, USA

Karl Franzens University Graz, Institute of Chemistry, Analytical Chemistry, Graz, Austria

Applied Speciation and Consulting, LLC, 18804 Northcreek Parkway Bothell, USA

University Hygienic Laboratory, 2220 South Ankeny Blvd., Ankeny, USA

J. Anal. At. Spectrom., 2011,26, 1740-1745

DOI: 10.1039/C1JA10040H
Received 02 Feb 2011, Accepted 07 Apr 2011
First published online 16 May 2011

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A limited interlaboratory study for arsenic speciation analysis of whole blood was conducted in conjunction with the New York State Department of Health's (NYS DOH's) proficiency testing (PT) program for total arsenic in whole blood. Four laboratories were able to report values for up to five arsenic species in blood materials representing typical environmental concentrations. The arsenic species were very challenging to measure, due to the low concentrations (<MDL—9.5 μg L⁻¹). For most arsenic species, good agreement among the participants was observed and the consensus mean values obtained can be considered as the assigned target values for use as quality assurance materials in future analyses.

Abstract from Analytical Abstracts 2011

A limited interlaboratory study for arsenic speciation analysis of whole blood was conducted in conjunction with the New York State Department of Health's (NYS DOHapos;s) proficiency testing (PT) program for total arsenic in whole blood. Four laboratories were able to report values for up to five arsenic species in blood materials representing typical environmental concentrations. The arsenic species were very challenging to measure, due to the low concentrations (<MDL—9.5 µg L^–1). For most arsenic species, good agreement among the participants was observed and the consensus mean values obtained can be considered as the assigned target values for use as quality assurance materials in future analyses.

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Kanna Ito
Walter Goessler
Hakan Gürleyük
Brian Wels
Christopher D. Palmer
Mary Frances Verostek
Patrick J. Parsons

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