Issue 7, 2011
From the journal:

Dalton Transactions

Borane-substituted imidazol-2-ylidenes: syntheses in vacuo

Alasdair W. Taylor,a   Kevin R. J. Lovelock,a   Robert G. Jonesa  and  Peter Licence*a  

* Corresponding authors

a School of Chemistry, The University of Nottingham, University Park, Nottingham, UK
E-mail: peter.licence@nottingham.ac.uk
Fax: +44 115 951 3058
Tel: +44 115 846 6176

Abstract

The serendipitous discovery of an efficient reactive distillation is reported. Two borane-substituted imidazol-2-ylidenes have been prepared in high yield from precursor tetrafluoroborate derived room temperature ionic liquids by reactive distillation at T > 500 K and p < 1 × 10−4 mbar.

Graphical abstract: Borane-substituted imidazol-2-ylidenes: syntheses in vacuo

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Article information

DOI
https://doi.org/10.1039/C0DT01240H
Article type
Paper
Submitted
15 Sep 2010
Accepted
18 Nov 2010
First published
12 Jan 2011

Dalton Trans., 2011,40, 1463-1470

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Borane-substituted imidazol-2-ylidenes: syntheses in vacuo

A. W. Taylor, K. R. J. Lovelock, R. G. Jones and P. Licence, Dalton Trans., 2011, 40, 1463 DOI: 10.1039/C0DT01240H

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