Boron and nitrogen-rich carbons from ionic liquid precursors with tailorable surface properties

Pasquale F. Fulvio; Je Seung Lee; Richard T. Mayes; Xiqing Wang; Shannon M. Mahurin; Sheng Dai

doi:10.1039/C1CP20631A

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Physical Chemistry Chemical Physics

Issue 30, 2011

High quality research in physical chemistry, chemical physics and biophysical chemistry.

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Boron and nitrogen-rich carbons from ionic liquid precursors with tailorable surface properties

Pasquale F. Fulvio,^a Je Seung Lee,*^a^b Richard T. Mayes,^a Xiqing Wang,^a Shannon M. Mahurin^a and Sheng Dai*^a

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Chemical Sciences Division, Oak Ridge National Laboratory, 1 Bethel Valley Road, Oak Ridge, USA
E-mail: dais@ornl.gov ;
Fax: +1 865 576 5235 ;
Tel: +1 865 576 7307

Department of Chemistry, Kyung Hee University, 1 Hoegi-dong, Dongdaemoon-gu, Seoul 130-701, Korea
E-mail: leejs70@khu.ac.kr ;
Fax: +82 2 966 3701 ;
Tel: +82 2 961 0458

Phys. Chem. Chem. Phys., 2011,13, 13486-13491

DOI: 10.1039/C1CP20631A
Received 05 Mar 2011, Accepted 12 Apr 2011
First published online 13 May 2011

This article is part of themed collection: Nanostructures in Ionic Liquids

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Abstract
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A novel strategy for tailoring the adsorption and structural properties of ionic liquid derived carbons has been developed. By changing the carbonization temperature and ratios of ionic liquids (ILs) containing a cross-linkable anion, such as 1-butyl-3-methylimidazolium tricyanomethanide [BMIm][C(CN)₃] and 1-ethyl-3-methylimidazolium tetracyanoborate [EMIm][B(CN)₄], boron and nitrogen-rich carbons with slit-like pores and specific surface areas exceeding 500 m² g⁻¹ have been prepared. Furthermore, the nitrogen-rich carbons exhibit high adsorption capacity for CO₂ adsorption and selectivity for CO₂/N₂ separation.

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Richard T. Mayes
Xiqing Wang
Shannon M. Mahurin
Sheng Dai

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