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Issue 29, 2011
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Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

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Abstract

Preparation of the all-syn isomer of 1,2,3,4-tetrafluorocyclohexane is reported; X-ray structural studies shows a conformation with two of the C–F bonds oriented 1,3-diaxial to each other and 19F-NMR reveals a through space diaxial 4JFF coupling constant of 29 Hz.

Graphical abstract: Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

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Publication details

The article was received on 23 May 2011, accepted on 14 Jun 2011 and first published on 28 Jun 2011


Article type: Communication
DOI: 10.1039/C1CC13016A
Citation: Chem. Commun., 2011,47, 8265-8267
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    Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

    A. J. Durie, A. M. Z. Slawin, T. Lebl, P. Kirsch and D. O'Hagan, Chem. Commun., 2011, 47, 8265
    DOI: 10.1039/C1CC13016A

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