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Issue 24, 2011
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Observing 13C–13C connectivities at high magnetic fields and very high spinning frequencies

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Abstract

We report the application of a dipolar recoupling sequence for the observation of 13C–13C connectivities in biomolecules at high magnetic fields (B0 ≥ 21.1 T) and ultra-high magic angle spinning frequencies (νR = 60 kHz). The efficiency and the robustness of this double-quantum technique are demonstrated on the YajG protein (19.6 kDa).

Graphical abstract: Observing 13C–13C connectivities at high magnetic fields and very high spinning frequencies

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Publication details

The article was received on 25 Mar 2011, accepted on 04 May 2011 and first published on 18 May 2011


Article type: Communication
DOI: 10.1039/C1CC11705J
Citation: Chem. Commun., 2011,47, 6930-6932
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    Observing 13C–13C connectivities at high magnetic fields and very high spinning frequencies

    O. Lafon, J. Trébosc, B. Hu, G. D. Paëpe and J. Amoureux, Chem. Commun., 2011, 47, 6930
    DOI: 10.1039/C1CC11705J

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