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Issue 20, 2011
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Iron oxide mediated direct C–H arylation/alkylation at α-position of cyclic aliphatic ethers

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Abstract

We report a new and efficient iron oxide catalyzed cross-coupling reaction between organometallic species such as alkyl/arylmagnesium halides or organolithium species and α-hydrogen bearing cyclic aliphatic ethersviaactivation of C(sp3)–H. This is the first example of iron oxide mediated direct C–C bond formation without expensive or toxic ligands.

Graphical abstract: Iron oxide mediated direct C–H arylation/alkylation at α-position of cyclic aliphatic ethers

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Publication details

The article was received on 24 Feb 2011, accepted on 29 Mar 2011 and first published on 18 Apr 2011


Article type: Communication
DOI: 10.1039/C1CC11094B
Citation: Chem. Commun., 2011,47, 5852-5854
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    Iron oxide mediated direct C–H arylation/alkylation at α-position of cyclic aliphatic ethers

    P. P. Singh, S. Gudup, S. Ambala, U. Singh, S. Dadhwal, B. Singh, S. D. Sawant and R. A. Vishwakarma, Chem. Commun., 2011, 47, 5852
    DOI: 10.1039/C1CC11094B

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