Issue 3, 2011
From the journal:

Chemical Communications

Designed synthesis of TS-1 crystals with controllable b-oriented length†

Zhichao Shan,b   Hong Wang,c   Xiangju Meng,*a   Siyu Liu,b   Liang Wang,b   Chunyu Wang,b   Fei Li,b   James P. Lewisc  and  Feng-Shou Xiao*a  

* Corresponding authors

a Key Lab of Applied Chemistry of Zhejiang Province, Department of Chemistry, Zhejiang University (XiXi Campus), Hangzhou 310028, P. R. China
E-mail: fsxiao@mail.jlu.edu.cn

b State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, China

c Department of Mechanical and Aerospace Engineering, West Virginia University, Morgantown, West Virginia 26506-6106, USA

Abstract

TS-1 crystals with controllable b-oriented length (sheet-like morphology, TS-1-S; chain-like morphology, TS-1-C) have been rationally synthesized from addition of organic additives (urea and fluorinated surfactant of FC-4) in the starting titanosilicate gels, and catalytic and adsorptive measurements show that TS-1-S samples are very active in Beckmann rearrangement of cyclohexanone oxime, whereas TS-1-C samples are selective in adsorption for para-xylene.

Graphical abstract: Designed synthesis of TS-1 crystals with controllable b-oriented length

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Article information

DOI
https://doi.org/10.1039/C0CC03613G
Article type
Communication
Submitted
02 Sep 2010
Accepted
18 Oct 2010
First published
15 Nov 2010

Chem. Commun., 2011,47, 1048-1050

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Designed synthesis of TS-1 crystals with controllable b-oriented length

Z. Shan, H. Wang, X. Meng, S. Liu, L. Wang, C. Wang, F. Li, J. P. Lewis and F. Xiao, Chem. Commun., 2011, 47, 1048 DOI: 10.1039/C0CC03613G

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