Jump to main content
Jump to site search

Issue 7, 2011
Previous Article Next Article

A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

Author affiliations

Abstract

We propose using singly-tuned μ-coils and 1H-detection to obtain high-sensitivity in lieu of miniaturizing cumbersome multi-resonance circuits, with the existing MAS probe circuitry/coil providing RF at other frequencies. We demonstrate two key building blocks in solid-state NMR: cross-polarization and heteronuclear decoupling. As well, a 1H-detected 2D HMQC is obtained.

Graphical abstract: A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

Back to tab navigation

Supplementary files

Publication details

The article was received on 25 Oct 2010, accepted on 02 Dec 2010 and first published on 23 Dec 2010


Article type: Communication
DOI: 10.1039/C0CC04607H
Citation: Chem. Commun., 2011,47, 2119-2121
  •   Request permissions

    A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

    P. M. Aguiar, J. Jacquinot and D. Sakellariou, Chem. Commun., 2011, 47, 2119
    DOI: 10.1039/C0CC04607H

Search articles by author

Spotlight

Advertisements