A synthesis of oligomeric α-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers

Kamyar Afarinkia; Martin Royappa; Ian J. Scowen; Jonathan W. Steed; Hiu-wan Yu

doi:10.1039/B917737J

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Organic & Biomolecular Chemistry

Issue 3, 2010

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A synthesis of oligomeric α-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers

Kamyar Afarinkia , Martin Royappa , Ian J. Scowen , Jonathan W. Steed and Hiu-wan Yu

Org. Biomol. Chem., 2010, 8, 600-606

DOI: 10.1039/B917737J
Received 28 Aug 2009, Accepted 30 Oct 2009
First published on the web 03 Dec 2009

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A general method for the synthesis of a novel class of oligomers, comprising α-hydroxy phenylphosphinic acid building blocks, is reported. A series of dimeric α-hydroxy phenylphosphinates are analyzed by a combination of NMR spectroscopy, X-ray crystallography and computational methods.

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Kamyar Afarinkia
Martin Royappa
Ian J. Scowen
Jonathan W. Steed
Hiu-wan Yu

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Organic & Biomolecular Chemistry

A synthesis of oligomeric α-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers

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