The Ames Laboratory, U.S. Department of Energy (OD JWW VKP) and Department of Materials Science and Engineering (VKP), Iowa State University, Ames, USA
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Aldrich Materials Science, Sigma-Aldrich Corporation, 6000 N. Teutonia Avenue, Milwaukee, USA
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New J. Chem., 2010,34, 25-28
23 Oct 2009,
04 Nov 2009
First published online
24 Nov 2009
The solvent-free reaction between o-vanillin and p-toluidine was investigated using NMR, DSC and XRD analyses. At room temperature, o-vanillin and p-toluidine react in a liquid eutectic formed upon grinding, while below 10 °C the same materials appear to react without the formation of a liquid phase, which most likely remains hidden behind solid reactants and reaction products.
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