Issue 9, 2010
From the journal:

Journal of Analytical Atomic Spectrometry

Real time monitoring of chemical transformations during catalyticreduction using gas source mass spectrometry: carbon/zinc carbonate hydroxide†

Anil Gopala,a   Norbert Jakubowski,a   Ulrich Panneab  and  Heinrich Kipphardt*a  

* Corresponding authors

a BAM Federal Institute for Materials Research and Testing, Richard-Willstaetter-Str. 11, Berlin, Germany
E-mail: heinrich.kipphardt@bam.de
Fax: +49 30 8104 1117
Tel: +49 30 8104 1116

b Humboldt-Universitaet zu Berlin, Department of Chemistry, Brook-Taylor-Strasse 2, Berlin, Germany

Abstract

We report herein the utilization of a vacuum reduction distillation system (VRDS) coupled with mass spectrometry (MS) to characterize chemical transformations in thermal analysis. The system initially designed to monitor metal purification by distillation is applied for the first time to the catalytic reaction of in situ formed nickel oxide during the carbothermic reduction of zinc oxide.1

Graphical abstract: Real time monitoring of chemical transformations during catalytic reduction using gas source mass spectrometry: carbon/zinc carbonate hydroxide

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Article information

DOI
https://doi.org/10.1039/C004179C
Article type
Communication
Submitted
11 Mar 2010
Accepted
18 Jun 2010
First published
02 Jul 2010

J. Anal. At. Spectrom., 2010,25, 1378-1380

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Real time monitoring of chemical transformations during catalytic reduction using gas source mass spectrometry: carbon/zinc carbonate hydroxide

A. Gopala, N. Jakubowski, U. Panne and H. Kipphardt, J. Anal. At. Spectrom., 2010, 25, 1378 DOI: 10.1039/C004179C

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