3D MnII coordination polymer with alternating azide/azide/formate/formate bridged chains: synthesis, structure and magnetic properties

Jiong-Peng Zhao; Bo-Wen Hu; Qian Yang; Xiao-Feng Zhang; Tong-Liang Hu; Xian-He Bu

doi:10.1039/B919048A

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Dalton Transactions

Issue 1, 2010

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3D Mn^II coordination polymer with alternating azide/azide/formate/formate bridged chains: synthesis, structure and magnetic properties

Jiong-Peng Zhao , Bo-Wen Hu , Qian Yang , Xiao-Feng Zhang , Tong-Liang Hu and Xian-He Bu

Dalton Trans., 2010, 39, 56-58

DOI: 10.1039/B919048A
Received 14 Sep 2009, Accepted 12 Oct 2009
First published on the web 28 Oct 2009

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A new 3D Mn^II coordination polymer, [Mn₂(HCO₂)(L)₂(N₃)·MeOH]_∞ (1) (L = nicotinate N-oxide), was synthesized by a solvothermal reaction and characterized magnetically. Complex 1 is a typical antiferromagnet with alternating azide/azide/formate/formate bridges, exhibiting a new –J₁J₁J₂J₂– coupling sequence. This is the first complex to contain an azide, formate and another type of carboxylate ligand.

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Jiong-Peng Zhao
Bo-Wen Hu
Qian Yang
Xiao-Feng Zhang
Tong-Liang Hu
Xian-He Bu

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Dalton Transactions

3D Mn^II coordination polymer with alternating azide/azide/formate/formate bridged chains: synthesis, structure and magnetic properties

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