Versatile assembly of p-carboxylatocalix[4]arene-O-alkyl ethers

Stuart Kennedy; Simon J. Teat; Scott J. Dalgarno

doi:10.1039/B914133B

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Dalton Transactions

Issue 2, 2010

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Versatile assembly of p-carboxylatocalix[4]arene-O-alkyl ethers

Stuart Kennedy , Simon J. Teat and Scott J. Dalgarno

Dalton Trans., 2010, 39, 384-387

DOI: 10.1039/B914133B
Received 15 Jul 2009, Accepted 30 Sep 2009
First published on the web 28 Oct 2009
This article is part of the collection: New Talent: Inspiration for the future

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Abstract
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Crystallisation of lower-rim tetra-O-alkylated p-carboxylatocalix[4]arenes from pyridine results in the formation of both bi-layer and pillar type supramolecular motifs. Full alkylation at the calixarene lower rim has significant influence over the supramolecular self-assembly motif, including preclusion of pyridine guest molecules from the calixarene cavity in the solid state.

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Additional unit cells for 8·Py and 9·Py to confirm bulk materialcomposition
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Dalton Transactions

Versatile assembly of p-carboxylatocalix[4]arene-O-alkyl ethers

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