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Issue 46, 2010
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Continuous-flow synthesis of vitamin D3

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Abstract

A highly efficient, two-stage, continuous-flow synthesis of vitamin D3 from provitamin D3 was achieved. The developed method afforded the desired product in high yield (HPLC-UV: 60%, isolated: 32%) and required neither intermediate purification nor high-dilution conditions.

Graphical abstract: Continuous-flow synthesis of vitamin D3

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Publication details

The article was received on 30 Jun 2010, accepted on 02 Sep 2010 and first published on 28 Sep 2010


Article type: Communication
DOI: 10.1039/C0CC02239J
Citation: Chem. Commun., 2010,46, 8722-8724
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    Continuous-flow synthesis of vitamin D3

    S. Fuse, N. Tanabe, M. Yoshida, H. Yoshida, T. Doi and T. Takahashi, Chem. Commun., 2010, 46, 8722
    DOI: 10.1039/C0CC02239J

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