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Issue 19, 2010
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A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC

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Abstract

A robust, versatile and easy to optimize HMBC experiment for complex organic structure elucidation which has been experimentally tested on cholesteryl acetate, cyclosporine and isopropylidene glycerol is described. The proposed experiment, IMPACT-HMBC (improved and accelerated constant-time heteronuclear multiple-bond correlation), combines sensitivity, easy experimental setup and can be recorded with short recovery times.

Graphical abstract: A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC

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Publication details

The article was received on 14 Jan 2010, accepted on 10 Mar 2010 and first published on 01 Apr 2010


Article type: Communication
DOI: 10.1039/C000964D
Citation: Chem. Commun., 2010,46, 3396-3398
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    A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC

    J. Furrer, Chem. Commun., 2010, 46, 3396
    DOI: 10.1039/C000964D

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