Total synthesis of largamide H

Shuo Liang; Zhengshuang Xu; Tao Ye

doi:10.1039/B921000H

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Chemical Communications

Issue 1, 2010

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Total synthesis of largamide H

Shuo Liang , Zhengshuang Xu and Tao Ye

Chem. Commun., 2010, 46, 153-155

DOI: 10.1039/B921000H
Received 07 Oct 2009, Accepted 29 Oct 2009
First published on the web 16 Nov 2009

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Total synthesis of largamide H has been completed, utilising the oxidative elimination reaction of enantiomerically pure 2-amino-3-(phenylselenyl)butanoic acid residues to stereospecifically install both (Z)- and (E)-2,3-dehydro-2-aminobutanoic moieties.

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Supplementary Info

Full details for experimental procedures for compounds 1, 3–5, 7–10, 12, 14, 15 and 17, and ¹H and ¹³C NMR spectra for compounds 1, 3–4, 5b, 7–9, 10a, 12, 14, 15b and 17
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Chemical Communications

Total synthesis of largamide H

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