Simultaneous production of p-tolualdehyde and hydrogen peroxide in photocatalytic oxygenation of p-xylene and reduction of oxygen with 9-mesityl-10-methylacridinium ion derivatives

Kei Ohkubo; Kentaro Mizushima; Ryosuke Iwata; Kazunori Souma; Nobuo Suzuki; Shunichi Fukuzumi

doi:10.1039/B920606J

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Chemical Communications

Issue 4, 2010

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Simultaneous production of p-tolualdehyde and hydrogen peroxide in photocatalytic oxygenation of p-xylene and reduction of oxygen with 9-mesityl-10-methylacridinium ion derivatives

Kei Ohkubo , Kentaro Mizushima , Ryosuke Iwata , Kazunori Souma , Nobuo Suzuki and Shunichi Fukuzumi

Chem. Commun., 2010, 46, 601-603

DOI: 10.1039/B920606J
Received 05 Oct 2009, Accepted 04 Nov 2009
First published on the web 18 Nov 2009

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Photooxygenation of p-xylene by oxygen occurs efficiently under photoirradiation of 9-mesityl-2,7,10-trimethylacridinium ion (Me₂Acr⁺–Mes) to yield p-tolualdehyde and hydrogen peroxide, which is initiated via photoinduced electron transfer of Me₂Acr⁺–Mes to produce the electron-transfer state.

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Kei Ohkubo
Kentaro Mizushima
Ryosuke Iwata
Kazunori Souma
Nobuo Suzuki
Shunichi Fukuzumi

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Chemical Communications

Simultaneous production of p-tolualdehyde and hydrogen peroxide in photocatalytic oxygenation of p-xylene and reduction of oxygen with 9-mesityl-10-methylacridinium ion derivatives

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