Molecular tectonics: crystal engineering of mixed valence Fe(II)/Fe(III) solid solutions

Pierre Dechambenoit; Sylvie Ferlay; Nathalie Kyritsakas; Mir Wais Hosseini

doi:10.1039/B919478A

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Chemical Communications

Issue 6, 2010

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Molecular tectonics: crystal engineering of mixed valence Fe(II)/Fe(III) solid solutions

Pierre Dechambenoit , Sylvie Ferlay , Nathalie Kyritsakas and Mir Wais Hosseini

Chem. Commun., 2010, 46, 868-870

DOI: 10.1039/B919478A
Received 18 Sep 2009, Accepted 13 Nov 2009
First published on the web 30 Nov 2009

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Abstract
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Based on isostructurality between crystals formed upon combining the dicationic tecton 2 with either M₃Fe^III(CN)₆ or M₄Fe^II(CN)₆ (M = Cs), a rare example of an H-bonded mixed valence Fe(II)–Fe(III) solid solution ((Cs₂2₃-[Fe^II(CN)₆]₂)_0.83(2₃-[Fe^III(CN)₆]₂)_0.17)) and curious necklace-like composite crystals were generated.

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Chemical Communications

Molecular tectonics: crystal engineering of mixed valence Fe(II)/Fe(III) solid solutions

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