A short, unsupported Cu(I)Cu(I) interaction, 2.65 Å, in a dinuclear guanidine chloride complex

Gina M. Chiarella; Doris Y. Melgarejo; Alex Rozanski; Pierre Hempte; Lisa M. Perez; Christian Reber; John P. Fackler Jr.

doi:10.1039/B918912B

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Chemical Communications

Issue 1, 2010

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A short, unsupported Cu(I)Cu(I) interaction, 2.65 Å, in a dinuclear guanidine chloride complex

Gina M. Chiarella , Doris Y. Melgarejo , Alex Rozanski , Pierre Hempte , Lisa M. Perez , Christian Reber and John P. Fackler Jr.

Chem. Commun., 2010, 46, 136-138

DOI: 10.1039/B918912B
Received 14 Sep 2009, Accepted 28 Oct 2009
First published on the web 13 Nov 2009

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Abstract
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The reaction of CuCl with the neutral guanidine Hhpp ligand (1,3,4,6,7,8-hexahydropyrimido[1,2-a]pyrimidine) yields two crystalline polymorphs of the neutral dimer, bis(1,3,4,6,7,8-hexahydropyrimido[1,2-a]pyrimidine) dichloro-di-copper(I) with the shortest distance known for a bridging unsupported copper(I)–copper(I) interaction.

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Articles By

Gina M. Chiarella
Doris Y. Melgarejo
Alex Rozanski
Pierre Hempte
Lisa M. Perez
Christian Reber
John P. Fackler Jr.

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Chemical Communications

A short, unsupported Cu(I)Cu(I) interaction, 2.65 Å, in a dinuclear guanidine chloride complex

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