Increasing the hydrophobicity and electrospray response of glycans through derivatization with novel cationic hydrazides

Michael S. Bereman; Daniel L. Comins; David C. Muddiman

doi:10.1039/B915589A

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Chemical Communications

Issue 2, 2010

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Increasing the hydrophobicity and electrospray response of glycans through derivatization with novel cationic hydrazides

Michael S. Bereman , Daniel L. Comins and David C. Muddiman

Chem. Commun., 2010, 46, 237-239

DOI: 10.1039/B915589A
Received 30 Jul 2009, Accepted 04 Nov 2009
First published on the web 17 Nov 2009

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Novel tags are used to increase the hydrophobicity of glycans and impart a permanent charge yielding as great as a [similar] 5-fold increase in electrospray response from both a standard and complex mixture.

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An experimental section describing synthesis of reagents 1 and 2 is given. In addition corresponding spectral data forreagents 1 and 2 are provided
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Chemical Communications

Increasing the hydrophobicity and electrospray response of glycans through derivatization with novel cationic hydrazides

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