Ortho-C–H borylation of benzoate esters with bis(pinacolato)diboron catalyzed by iridium–phosphine complexes

Tatsuo Ishiyama; Hironori Isou; Takao Kikuchi; Norio Miyaura

doi:10.1039/B910298A

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Chemical Communications

Issue 1, 2010

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Ortho-C–H borylation of benzoate esters with bis(pinacolato)diboron catalyzed by iridium–phosphine complexes

Tatsuo Ishiyama , Hironori Isou , Takao Kikuchi and Norio Miyaura

Chem. Commun., 2010, 46, 159-161

DOI: 10.1039/B910298A
Received 26 May 2009, Accepted 03 Nov 2009
First published on the web 17 Nov 2009

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Iridium complexes generated from [Ir(OMe)(COD)]₂ and tris[3,5-bis(trifluoromethyl)phenyl]phosphine efficiently catalyzed the ortho-C–H borylation of benzoate esters with bis(pinacolato)diboron in octane at 80 °C to produce the corresponding arylboronates in high yields with excellent regioselectivities.

Abstract from Catalysts & Catalysed Reactions 2010

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Chemical Communications

Ortho-C–H borylation of benzoate esters with bis(pinacolato)diboron catalyzed by iridium–phosphine complexes

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