Issue 43, 2010

Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

Abstract

Perdeuterated poly(acrylonitrile) is introduced as a practically proton-free alignment medium for the measurement of anisotropic NMR parameters; its use in conventional glass tubes and in a Kalrez® 8002 UP-based stretching device with resulting spectra of astonishing quality are demonstrated.

Graphical abstract: Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

Supplementary files

Article information

Article type
Communication
Submitted
22 Jul 2010
Accepted
09 Sep 2010
First published
30 Sep 2010

Chem. Commun., 2010,46, 8273-8275

Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

G. Kummerlöwe, M. Behl, A. Lendlein and B. Luy, Chem. Commun., 2010, 46, 8273 DOI: 10.1039/C0CC02730H

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