Issue 43, 2010
From the journal:

Chemical Communications

Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium†

Grit Kummerlöwe,a   Marc Behl,b   Andreas Lendleinb  and  Burkhard Luy*c  

* Corresponding authors

a Institut für Biologische Grenzflächen 2, Karlsruher Institut für Technologie, Herrmann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen, Germany

b GKSS Research Center GmbH, Kantstr. 55, 14513 Teltow, Germany

c Institut für Organische Chemie, Karlsruher Institut für Technologie, Fritz-Haber-Weg 6, 76131 Karlsruhe, Germany
E-mail: Burkhard.Luy@kit.edu
Tel: +49 721 608 5354

Abstract

Perdeuterated poly(acrylonitrile) is introduced as a practically proton-free alignment medium for the measurement of anisotropic NMR parameters; its use in conventional glass tubes and in a Kalrez® 8002 UP-based stretching device with resulting spectra of astonishing quality are demonstrated.

Graphical abstract: Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

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Article information

DOI
https://doi.org/10.1039/C0CC02730H
Article type
Communication
Submitted
22 Jul 2010
Accepted
09 Sep 2010
First published
30 Sep 2010

Chem. Commun., 2010,46, 8273-8275

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Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

G. Kummerlöwe, M. Behl, A. Lendlein and B. Luy, Chem. Commun., 2010, 46, 8273 DOI: 10.1039/C0CC02730H

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