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Issue 43, 2010
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Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

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Abstract

Perdeuterated poly(acrylonitrile) is introduced as a practically proton-free alignment medium for the measurement of anisotropic NMR parameters; its use in conventional glass tubes and in a Kalrez® 8002 UP-based stretching device with resulting spectra of astonishing quality are demonstrated.

Graphical abstract: Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

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Publication details

The article was received on 22 Jul 2010, accepted on 09 Sep 2010 and first published on 30 Sep 2010


Article type: Communication
DOI: 10.1039/C0CC02730H
Citation: Chem. Commun., 2010,46, 8273-8275
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    Artifact-free measurement of residual dipolar couplings in DMSO by the use of cross-linked perdeuterated poly(acrylonitrile) as alignment medium

    G. Kummerlöwe, M. Behl, A. Lendlein and B. Luy, Chem. Commun., 2010, 46, 8273
    DOI: 10.1039/C0CC02730H

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