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Issue 27, 2010
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Direct observation of a transient polymorph during crystallization

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Abstract

Application of a technique developed for in situ solid-state 13C NMR studies of crystallization processes reveals direct evidence that crystallization of glycine from a methanol/water solution involves the initial transient formation of the β polymorph, which then undergoes a solution-mediated polymorphic transformation to yield the more stable α polymorph.

Graphical abstract: Direct observation of a transient polymorph during crystallization

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Publication details

The article was received on 18 Apr 2010, accepted on 10 May 2010 and first published on 27 May 2010


Article type: Communication
DOI: 10.1039/C0CC01007C
Citation: Chem. Commun., 2010,46, 4982-4984
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    Direct observation of a transient polymorph during crystallization

    C. E. Hughes and K. D. M. Harris, Chem. Commun., 2010, 46, 4982
    DOI: 10.1039/C0CC01007C

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