Issue 25, 2010

On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

Abstract

We report the use of a nanolitre nuclear magnetic resonance (NMR) spectroscopy microfluidic chip hyphenated to a continuous-flow microlitre-microwave irradiation set-up, for on-line monitoring and rapid optimization of reaction conditions.

Graphical abstract: On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

Supplementary files

Article information

Article type
Communication
Submitted
26 Nov 2009
Accepted
16 Apr 2010
First published
25 May 2010

Chem. Commun., 2010,46, 4514-4516

On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

M. V. Gomez, H. H. J. Verputten, A. Díaz-Ortíz, A. Moreno, A. de la Hoz and A. H. Velders, Chem. Commun., 2010, 46, 4514 DOI: 10.1039/B924936B

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