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Issue 25, 2010
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On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

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Abstract

We report the use of a nanolitre nuclear magnetic resonance (NMR) spectroscopy microfluidic chip hyphenated to a continuous-flow microlitre-microwave irradiation set-up, for on-line monitoring and rapid optimization of reaction conditions.

Graphical abstract: On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

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Publication details

The article was received on 26 Nov 2009, accepted on 16 Apr 2010 and first published on 25 May 2010


Article type: Communication
DOI: 10.1039/B924936B
Citation: Chem. Commun., 2010,46, 4514-4516
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    On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

    M. V. Gomez, H. H. J. Verputten, A. Díaz-Ortíz, A. Moreno, A. de la Hoz and A. H. Velders, Chem. Commun., 2010, 46, 4514
    DOI: 10.1039/B924936B

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