Issue 25, 2010
From the journal:

Chemical Communications

On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy†

M. Victoria Gomez,a   Hein H. J. Verputten,b   Angel Díaz-Ortíz,a   Andres Moreno,a   Antonio de la Hoz*a  and  Aldrik H. Velders*b  

* Corresponding authors

a Instituto Regional de Investigación Científica Aplicada (IRICA), Universidad de Castilla-La Mancha, 13071 Ciudad Real, Spain
E-mail: Antonio.Hoz@uclm.es
Fax: 34 9022 04130
Tel: 34 9022 04100

b NMR & MS Department, MESA+ Institute for Nanotechnology, Faculty of Science and Technology, University of Twente, Enschede, The Netherlands
E-mail: a.h.velders@utwente.nl
Fax: 31 53489 4645
Tel: 31 53489 2980

Abstract

We report the use of a nanolitre nuclear magnetic resonance (NMR) spectroscopy microfluidic chip hyphenated to a continuous-flow microlitre-microwave irradiation set-up, for on-line monitoring and rapid optimization of reaction conditions.

Graphical abstract: On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

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Article information

DOI
https://doi.org/10.1039/B924936B
Article type
Communication
Submitted
26 Nov 2009
Accepted
16 Apr 2010
First published
25 May 2010

Chem. Commun., 2010,46, 4514-4516

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On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy

M. V. Gomez, H. H. J. Verputten, A. Díaz-Ortíz, A. Moreno, A. de la Hoz and A. H. Velders, Chem. Commun., 2010, 46, 4514 DOI: 10.1039/B924936B

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