Highly enantioselective synthesis of angelmarin

Hang Jiang; Yasumasa Hamada

doi:10.1039/B913400J

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Organic & Biomolecular Chemistry

Issue 20, 2009

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Highly enantioselective synthesis of angelmarin

Hang Jiang and Yasumasa Hamada

Org. Biomol. Chem., 2009, 7, 4173-4176

DOI: 10.1039/B913400J
Received 06 Jul 2009, Accepted 23 Jul 2009
First published on the web 04 Aug 2009

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Angelmarin (1), a novel anti-cancer agent, was efficiently synthesized through a highly enantioselective epoxidation and a copper cyanide-mediated esterification of the hindered alcohol as the key steps in 53% overall yield.

Abstract from Natural Product Updates 2010

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Supplementary Info

Experimental and NMR data of compounds; copies of ¹H NMR and ¹³C NMR spectra of compounds
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Organic & Biomolecular Chemistry

Highly enantioselective synthesis of angelmarin

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