Controllable stereoselective synthesis of trisubstituted alkenes by a catalytic three-component reaction of terminal alkynes, benzylic alcohols, and simple arenes

Hai-Hua Li; Yin-Huan Jin; Jie-Qi Wang; Shi-Kai Tian

doi:10.1039/B911954J

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Organic & Biomolecular Chemistry

Issue 16, 2009

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Controllable stereoselective synthesis of trisubstituted alkenes by a catalytic three-component reaction of terminal alkynes, benzylic alcohols, and simple arenes

Hai-Hua Li , Yin-Huan Jin , Jie-Qi Wang and Shi-Kai Tian

Org. Biomol. Chem., 2009, 7, 3219-3221

DOI: 10.1039/B911954J
Received 17 Jun 2009, Accepted 22 Jun 2009
First published on the web 30 Jun 2009

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The acid-catalyzed three-component reaction of terminal alkynes, benzylic alcohols, and simple arenes provides convenient and atom-economic access to an array of both Z- and E-isomers of trisubstituted alkenes with excellent stereoselectivity by switching reaction temperature and acidic catalysts.

Abstract from Catalysts & Catalysed Reactions 2009

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Supplementary Info

Experimental procedures, characterization data, and copies of¹H and ¹³C NMR spectra for the products
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Organic & Biomolecular Chemistry

Controllable stereoselective synthesis of trisubstituted alkenes by a catalytic three-component reaction of terminal alkynes, benzylic alcohols, and simple arenes

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