A concise total synthesis of (±)-acutifolone A

Ming-Tsang Hsieh; Hsing-Jang Liu; Tai Wei Ly; Kak-Shan Shia

doi:10.1039/B905910E

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Organic & Biomolecular Chemistry

Issue 16, 2009

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A concise total synthesis of (±)-acutifolone A

Ming-Tsang Hsieh , Hsing-Jang Liu , Tai Wei Ly and Kak-Shan Shia

Org. Biomol. Chem., 2009, 7, 3285-3290

DOI: 10.1039/B905910E
Received 24 Mar 2009, Accepted 21 May 2009
First published on the web 19 Jun 2009

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Starting from 4-methylcyclohexanone (7), a concise total synthesis of the pinguisane-type sesquiterpenoid acutifolone A, in racemic form, has been accomplished in 14 steps with an overall yield of 14.5%.

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Supplementary Info

¹H and ¹³C spectra for all new compounds and an X-raycrystallographical picture of 5a
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Crystal structure data
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Organic & Biomolecular Chemistry

A concise total synthesis of (±)-acutifolone A

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