Efficient use of the Dmab protecting group: applications for the solid-phase synthesis of N-linked glycopeptides

Trent Conroy; Katrina A. Jolliffe; Richard J. Payne

doi:10.1039/B821051A

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Organic & Biomolecular Chemistry

Issue 11, 2009

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Efficient use of the Dmab protecting group: applications for the solid-phase synthesis of N-linked glycopeptides

Trent Conroy , Katrina A. Jolliffe and Richard J. Payne

Org. Biomol. Chem., 2009, 7, 2255-2258

DOI: 10.1039/B821051A
Received 25 Nov 2008, Accepted 18 Mar 2009
First published on the web 26 Mar 2009

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Abstract
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An efficient protocol for the chemoselective removal of Dmab esters on the solid phase is reported; this method has been successfully utilised for the convergent solid phase synthesis of N-linked glycopeptides.

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Experimental details of SPPS and aspartylation protocols and characterisation of glycopeptides
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Organic & Biomolecular Chemistry

Efficient use of the Dmab protecting group: applications for the solid-phase synthesis of N-linked glycopeptides

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