Radical pairs with rotational fluidity in the photochemical reaction of acetophenone and cyclohexane in the zeolite NAY: a 13C CPMAS NMR and product analysis study

Ammee Amboya; Tina Nguyen; Hien T. Huynh; Ashley Brown; Gretchen Ratliff; Heather Yonutas; Deniz Cizmeciyan; Arunkumar Natarajan; Miguel A. Garcia Garibay

doi:10.1039/B815266G

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Organic & Biomolecular Chemistry

Issue 11, 2009

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Radical pairs with rotational fluidity in the photochemical reaction of acetophenone and cyclohexane in the zeolite NAY: a ¹³C CPMAS NMR and product analysis study

Ammee Amboya , Tina Nguyen , Hien T. Huynh , Ashley Brown , Gretchen Ratliff , Heather Yonutas , Deniz Cizmeciyan , Arunkumar Natarajan and Miguel A. Garcia Garibay

Org. Biomol. Chem., 2009, 7, 2322-2326

DOI: 10.1039/B815266G
Received 02 Sep 2008, Accepted 17 Feb 2009
First published on the web 16 Apr 2009

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The photochemical reaction of acetophenone and cyclohexane in the zeolite NaY occurs by combination of the geminate radical pairs to give products that reveal a significant amount of rotational fluidity, which was also documented by intermolecular nuclear dipolar interaction measurements using cross polarization ¹³C NMR (CPMAS) experiments.

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Ammee Amboya
Tina Nguyen
Hien T. Huynh
Ashley Brown
Gretchen Ratliff
Heather Yonutas
Deniz Cizmeciyan
Arunkumar Natarajan
Miguel A. Garcia Garibay

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Organic & Biomolecular Chemistry

Radical pairs with rotational fluidity in the photochemical reaction of acetophenone and cyclohexane in the zeolite NAY: a ¹³C CPMAS NMR and product analysis study

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