Capillary microreactors wall-coated with mesoporous titania thin film catalyst supports

Evgeny V. Rebrov; Angel Berenguer-Murcia; Helen E. Skelton; Brian F. G. Johnson; Andrew. E. H. Wheatley; Jaap C. Schouten

doi:10.1039/B815716B

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Lab on a Chip

Issue 4, 2009

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Capillary microreactors wall-coated with mesoporous titania thin film catalyst supports

Evgeny V. Rebrov , Angel Berenguer-Murcia , Helen E. Skelton , Brian F. G. Johnson , Andrew. E. H. Wheatley and Jaap C. Schouten

Lab Chip, 2009, 9, 503-506

DOI: 10.1039/B815716B
Received 09 Sep 2008, Accepted 31 Oct 2008
First published on the web 17 Nov 2008

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Abstract
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A new method for catalyst deposition on the inner walls of capillary microreactors is proposed which allows exact control of the coating thickness, pore size of the support, metal particle size, and metal loading. The wall-coated microreactors have been tested in a selective hydrogenation reaction. Activity and selectivity reach values close to those obtained with a homogeneous Pd catalyst. The catalyst activity was stable for a period of 1000 h time-on-stream.

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Supplementary Info

The detailed protocol for the preparation of the thin filmprecursor solution and high resolution transmission electronmicrographs of confined nanoparticles.
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Articles By

Evgeny V. Rebrov
Angel Berenguer-Murcia
Helen E. Skelton
Brian F. G. Johnson
Andrew. E. H. Wheatley
Jaap C. Schouten

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Capillary microreactors wall-coated with mesoporous titania thin film catalyst supports

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