A new homogeneous polymer support based on syndiotactic polystyrene and its application in palladium-catalyzed Suzuki–Miyaura cross-coupling reactions

Jihoon Shin; Julie Bertoia; Kenneth R. Czerwinski; Chulsung Bae

doi:10.1039/B913060H

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Green Chemistry

Issue 10, 2009

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A new homogeneous polymer support based on syndiotactic polystyrene and its application in palladium-catalyzed Suzuki–Miyaura cross-coupling reactions

Jihoon Shin , Julie Bertoia , Kenneth R. Czerwinski and Chulsung Bae

Green Chem., 2009, 11, 1576-1580

DOI: 10.1039/B913060H
Received 07 May 2009, Accepted 23 Jun 2009
First published on the web 17 Jul 2009

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Soluble syndiotactic polystyrene-supported triphenylphosphine (sPS–TPP) was synthesized by reacting borylated syndiotactic polystyrene with (4-bromophenyl)diphenylphosphine. A palladium catalyst, supported on sPS–TPP, effectively catalyzed Suzuki–Miyaura coupling reactions of aryl halides under homogeneous conditions. The polymer-supported palladium complex was recovered quantitatively by adding an equal volume of poor solvent to the polymer, and coupling products could be easily isolated by evaporating the solvents. The recovered polymer complex was reused several times without significant loss of activity.

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Green Chemistry

A new homogeneous polymer support based on syndiotactic polystyrene and its application in palladium-catalyzed Suzuki–Miyaura cross-coupling reactions

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