Long term continuous chemoenzymatic dynamic kinetic resolution of rac-1-phenylethanol using ionic liquids and supercritical carbon dioxide

Pedro Lozano; Teresa De Diego; Corina Mira; Kimberley Montague; Michel Vaultier; José L. Iborra

doi:10.1039/B821623A

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Green Chemistry

Issue 4, 2009

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Long term continuous chemoenzymatic dynamic kinetic resolution of rac-1-phenylethanol using ionic liquids and supercritical carbon dioxide

Pedro Lozano , Teresa De Diego , Corina Mira , Kimberley Montague , Michel Vaultier and José L. Iborra

Green Chem., 2009, 11, 538-542

DOI: 10.1039/B821623A
Received 02 Dec 2008, Accepted 19 Jan 2009
First published on the web 13 Feb 2009

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Abstract
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The long term continuous dynamic kinetic resolution (DKR) of rac-phenylethanol in IL/scCO₂ biphasic systems was carried out by simultaneously using immobilized lipase (Novozym 435) and acidic zeolite catalysts at 50 °C and 100 bar, providing good yields (up to 98.0%) for R-phenylethyl propionate with excellent enantioselectivity (up to 97.3% ee) and without any activity loss during 14 days of operation.

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Pedro Lozano
Teresa De Diego
Corina Mira
Kimberley Montague
Michel Vaultier
José L. Iborra

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Green Chemistry

Long term continuous chemoenzymatic dynamic kinetic resolution of rac-1-phenylethanol using ionic liquids and supercritical carbon dioxide

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