An efficient, practical and cost-effective polymer-supported catalyst for the transesterification of methyl methacrylate by 1-butanol

Gaëlle Baquey; Marie-Hélène Alvès; Magalie Graullier; Alain Riondel; Jean-Michel Paul; Marc Birot; Hervé Deleuze

doi:10.1039/B820704F

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Green Chemistry

Issue 6, 2009

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An efficient, practical and cost-effective polymer-supported catalyst for the transesterification of methyl methacrylate by 1-butanol

Gaëlle Baquey , Marie-Hélène Alvès , Magalie Graullier , Alain Riondel , Jean-Michel Paul , Marc Birot and Hervé Deleuze

Green Chem., 2009, 11, 868-872

DOI: 10.1039/B820704F
Received 19 Nov 2008, Accepted 12 Mar 2009
First published on the web 30 Mar 2009

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Abstract
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A straightforward and cost-effective synthesis of a polymer-supported titanium alkoxide catalyst is reported. The described synthesis involves cheap, readily available and relatively non toxic chemicals, solvents and workup procedures. Efficiency and stability of the catalyst were tested in a laboratory-scale continuous flow reactor under equilibrium conditions over a month period. The average daily titanium leaching was estimated to less than 1% of the total amount of titanium engaged. To our knowledge, this result is the best obtained, to date, concerning the use of heterogeneous titanate for the catalysis of transesterification reactions.

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Gaëlle Baquey
Marie-Hélène Alvès
Magalie Graullier
Alain Riondel
Jean-Michel Paul
Marc Birot
Hervé Deleuze

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Green Chemistry

An efficient, practical and cost-effective polymer-supported catalyst for the transesterification of methyl methacrylate by 1-butanol

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