Tetranuclear vanadium complex, (VO)4(hpic)4: a recyclable catalyst for oxidation of benzyl alcohols with molecular oxygen

Shintaro Kodama; Yukihiro Ueta; Jun Yoshida; Akihiro Nomoto; Shigenobu Yano; Michio Ueshima; Akiya Ogawa

doi:10.1039/B913823D

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Dalton Transactions

Issue 44, 2009

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Tetranuclear vanadium complex, (VO)₄(hpic)₄: a recyclable catalyst for oxidation of benzyl alcohols with molecular oxygen

Shintaro Kodama , Yukihiro Ueta , Jun Yoshida , Akihiro Nomoto , Shigenobu Yano , Michio Ueshima and Akiya Ogawa

Dalton Trans., 2009, 9708-9711

DOI: 10.1039/B913823D
Received 10 Jul 2009, Accepted 02 Sep 2009
First published on the web 15 Sep 2009

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Vanadium(IV) complexes bearing 3-hydroxypicolinic acid (H₂hpic) as ligands, VO(Hhpic)₂ (1) and the cyclic tetramer (VO)₄(hpic)₄ (2), have excellent catalytic ability for the oxidation of a variety of primary and secondary benzyl alcohols with molecular oxygen in acetonitrile or protic solvents such as ethanol and water, affording the corresponding aldehydes and ketones, respectively. Construction of multi-nuclear complexes by the selection of ligands attains higher turnover numbers and recycling of the catalyst.

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A review, with 32 references, providing an overview of the title catalysts in organic reactions.

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Shintaro Kodama
Yukihiro Ueta
Jun Yoshida
Akihiro Nomoto
Shigenobu Yano
Michio Ueshima
Akiya Ogawa

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Dalton Transactions

Tetranuclear vanadium complex, (VO)₄(hpic)₄: a recyclable catalyst for oxidation of benzyl alcohols with molecular oxygen

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