Syntheses, structures, and photoluminescence of 1-D lanthanide coordination polymers

Xiaoping Yang; Richard A. Jones; Joseph H. Rivers; Wai-Kwok Wong

doi:10.1039/B910588C

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Dalton Transactions

Issue 47, 2009

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Syntheses, structures, and photoluminescence of 1-D lanthanide coordination polymers

Xiaoping Yang , Richard A. Jones , Joseph H. Rivers and Wai-Kwok Wong

Dalton Trans., 2009, 10505-10510

DOI: 10.1039/B910588C
Received 29 May 2009, Accepted 15 Oct 2009
First published on the web 29 Oct 2009

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Abstract
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Five new lanthanide 1-D coordination polymers are reported which are formed from flexible salen type Schiff-base ligands H₂L and H₂L′ (H₂L = N,N¹-ethylene bis(salicylideneimine); H₂L′ = N,N¹-bis(3-methoxysalicylidene)ethylene-1,2-diamine). The polymeric structures are formed by bridging neutral H₂L units in the case of {[Ln₂L₂(CF₃SO₃)(H₂L)₄(MeOH)]·CF₃SO₃}_n (Ln = Eu (1), Nd (2) and Er (3)), and by acetate (OAc⁻) groups in [Yb₂(L)₂(OAc)₂(MeOH)₂]_n (4) and {[Tb₃(L′)₂(OAc)₅]·Et₂O·(MeOH)_0.5}_n (5). The structures of 1–5 were determined by single crystal X-ray crystallographic studies and the luminescence properties of 1 and 5 in MeOH solution were determined.

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Syntheses, structures, and photoluminescence of 1-D lanthanide coordination polymers

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