Issue 9, 2009
From the journal:

Dalton Transactions

The first thiosilicate from solution: synthesis and crystal structure of (NH4)2[SiS3(NH3)]·2NH3

Martin Meiera  and  Nikolaus Korber*a  

* Corresponding authors

a Institut für Anorganische Chemie, Universität Regensburg, 93040 Regensburg, Germany
E-mail: nikolaus.korber@chemie.uni-regensburg.de
Fax: +49 941 943 1812
Tel: +49 941 943 4448

Abstract

The ammonolysis of SiS2 in liquid ammonia yields crystalline (NH4)2[SiS3(NH3)]·2NH3, which contains [SiS3(NH3)]2− as a derivative of the ortho-thiosilicate anion SiS44−.

Graphical abstract: The first thiosilicate from solution: synthesis and crystal structure of (NH4)2[SiS3(NH3)]·2NH3

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Article information

DOI
https://doi.org/10.1039/B818856D
Article type
Communication
Submitted
24 Oct 2008
Accepted
24 Dec 2008
First published
09 Jan 2009

Dalton Trans., 2009, 1506-1508

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The first thiosilicate from solution: synthesis and crystal structure of (NH4)2[SiS3(NH3)]·2NH3

M. Meier and N. Korber, Dalton Trans., 2009, 1506 DOI: 10.1039/B818856D

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