Synthesis and structural studies of metallamacrotricycles based on a metacyclophane in 1,3-alternate conformation bearing four imidazolyl units

Jérôme Ehrhart; Jean-Marc Planeix; Nathalie Kyritsakas-Gruber; Mir Wais Hosseini

doi:10.1039/B816053H

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Dalton Transactions

Issue 14, 2009

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Synthesis and structural studies of metallamacrotricycles based on a metacyclophane in 1,3-alternate conformation bearing four imidazolyl units

Jérôme Ehrhart , Jean-Marc Planeix , Nathalie Kyritsakas-Gruber and Mir Wais Hosseini

Dalton Trans., 2009, 2552-2557

DOI: 10.1039/B816053H
Received 15 Sep 2008, Accepted 21 Jan 2009
First published on the web 12 Feb 2009

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Abstract
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The combination of a [1111]metacyclophane blocked in 1,3-alternate conformation and bearing four imidazole units with MX₂ (M = Co, Cu, Zn and Hg; X = Cl or Br) complexes leads to the formation of a series of analogous neutral metallamacrotricycles. In all cases, the structure of the binuclear complexes has been studied by X-ray diffraction methods on single crystals.

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Dalton Transactions

Synthesis and structural studies of metallamacrotricycles based on a metacyclophane in 1,3-alternate conformation bearing four imidazolyl units

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