Functionalised azetidines as ligands: pyridyl-complemented coordination

Young Hoon Lee; Jack Harrowfield; Yang Kim; Woo Taik Lim; Yu Cheol Park; Pierre Thuéry

doi:10.1039/B812295D

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Dalton Transactions

Issue 3, 2009

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Functionalised azetidines as ligands: pyridyl-complemented coordination

Young Hoon Lee , Jack Harrowfield , Yang Kim , Woo Taik Lim , Yu Cheol Park and Pierre Thuéry

Dalton Trans., 2009, 434-442

DOI: 10.1039/B812295D
Received 18 Jul 2008, Accepted 16 Sep 2008
First published on the web 13 Nov 2008

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Abstract
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A relatively simple azetidine derivative with 2-aminoethyl and 2-pyridyl substituents functions as a tridentate ligand towards Cu(II), giving species in which the CuN₃ unit is essentially planar and that, in the solid state, show a subtle balance between mononuclear and binuclear forms, allowing both to be simultaneously present in some lattices. Displacement of the ligand from Cu(II) by the use of cyanide results in the formation of cyanogen, which appears to slowly react with the free amine to give an oxamidine characterised in its doubly-deprotonated form as its binuclear Ni(II) complex.

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Young Hoon Lee
Jack Harrowfield
Yang Kim
Woo Taik Lim
Yu Cheol Park
Pierre Thuéry

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Dalton Transactions

Functionalised azetidines as ligands: pyridyl-complemented coordination

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