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Issue 44, 2009
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Double-quantum 19F–19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides

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Abstract

A broadband dipolar recoupling method robust to chemical shift is introduced to observe 19F–19F proximities in fluoroaluminates in high magnetic field and at ultra-fast magic angle spinning (>60 kHz).

Graphical abstract: Double-quantum 19F–19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides

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Publication details

The article was received on 17 Jul 2009, accepted on 28 Aug 2009 and first published on 23 Sep 2009


Article type: Paper
DOI: 10.1039/B914468D
Citation: Phys. Chem. Chem. Phys., 2009,11, 10391-10395
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    Double-quantum 19F–19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides

    Q. Wang, B. Hu, F. Fayon, J. Trébosc, C. Legein, O. Lafon, F. Deng and J. Amoureux, Phys. Chem. Chem. Phys., 2009, 11, 10391
    DOI: 10.1039/B914468D

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