Double-quantum 19F–19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides

Qiang Wang; Bingwen Hu; Franck Fayon; Julien Trébosc; Christophe Legein; Olivier Lafon; Feng Deng; Jean-Paul Amoureux

doi:10.1039/B914468D

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Physical Chemistry Chemical Physics

Issue 44, 2009

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Double-quantum ¹⁹F–¹⁹F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of ¹⁹F NMR spectra of inorganic fluorides

Qiang Wang , Bingwen Hu , Franck Fayon , Julien Trébosc , Christophe Legein , Olivier Lafon , Feng Deng and Jean-Paul Amoureux

Phys. Chem. Chem. Phys., 2009, 11, 10391-10395

DOI: 10.1039/B914468D
Received 17 Jul 2009, Accepted 28 Aug 2009
First published on the web 23 Sep 2009

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A broadband dipolar recoupling method robust to chemical shift is introduced to observe ¹⁹F–¹⁹F proximities in fluoroaluminates in high magnetic field and at ultra-fast magic angle spinning (>60 kHz).

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Qiang Wang
Bingwen Hu
Franck Fayon
Julien Trébosc
Christophe Legein
Olivier Lafon
Feng Deng
Jean-Paul Amoureux

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Physical Chemistry Chemical Physics

Double-quantum ¹⁹F–¹⁹F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of ¹⁹F NMR spectra of inorganic fluorides

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