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Issue 18, 2009
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Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

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Abstract

A new two-dimensional NMR experiment is described which is suitable for obtaining magic angle spinning (MAS) scalar correlation spectra in solids. The new experiment has several advantages, including increased cross peak intensities, coupled with good suppression of the diagonal. Its utility is demonstrated via assignments of the carbon-13 MAS spectra of progesterone at natural abundance and of the polymer phase of 50%-U-13C-CsC60.

Graphical abstract: Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

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Publication details

The article was received on 24 Oct 2008, accepted on 26 Jan 2009 and first published on 02 Mar 2009


Article type: Paper
DOI: 10.1039/B818867J
Citation: Phys. Chem. Chem. Phys., 2009,11, 3547-3553
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    Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

    D. Lee, J. Struppe, D. W. Elliott, L. J. Mueller and J. J. Titman, Phys. Chem. Chem. Phys., 2009, 11, 3547
    DOI: 10.1039/B818867J

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