Fe(II) spincrossover complex of [1,2,5]thiadiazolo[3,4-f][1,10]phenanthroline

Yoshiaki Shuku; Rie Suizu; Kunio Awaga; Osamu Sato

doi:10.1039/B906845G

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CrystEngComm

Issue 10, 2009

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Fe(II) spincrossover complex of [1,2,5]thiadiazolo[3,4-f][1,10]phenanthroline

Yoshiaki Shuku , Rie Suizu , Kunio Awaga and Osamu Sato

CrystEngComm, 2009, 11, 2065-2068

DOI: 10.1039/B906845G
Received 06 Apr 2009, Accepted 26 May 2009
First published on the web 11 Jun 2009
This article is part of the collection: Crystal engineering in molecular magnetism

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Abstract
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We prepared an iron(II) spin crossover complex with a new ligand, [1,2,5]thiadiazolo[3,4-f][1,10]phenanthroline, which is a 1,10-phenanthroline analogue annulated with a thiadiazole moiety. X-Ray crystal analysis indicated a 3D network structure formed by short SS contacts, and magnetic measurements revealed a broad transition above room temperature.

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Supplementary Info

Crystal structure data
CIF (142K)
Crystallographic data of 1·CH₂Cl₂ and 3 are summarized in Table S1 and the ORTEPdrawings of 1·CH₂Cl₂ and 3 are shown in Fig. S1 and S2
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Crystal structure data
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Fe(II) spincrossover complex of [1,2,5]thiadiazolo[3,4-f][1,10]phenanthroline

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