Crystal engineering of 5,5′-bisdiazo-dipyrromethane with halogenπ synthons

Zhenming Yin; Wuyan Wang; Miao Du; Xiuguang Wang; Jianhua Guo

doi:10.1039/B905568A

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CrystEngComm

Issue 11, 2009

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Crystal engineering of 5,5′-bisdiazo-dipyrromethane with halogenπ synthons

Zhenming Yin , Wuyan Wang , Miao Du , Xiuguang Wang and Jianhua Guo

CrystEngComm, 2009, 11, 2441-2446

DOI: 10.1039/B905568A
Received 19 Mar 2009, Accepted 08 Jul 2009
First published on the web 28 Jul 2009

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Abstract
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Chlorine, bromine and iodine substituted derivatives of 5,5′-bisdiazo-dipyrromethane have been synthesized and their crystal structures were studied by X-ray crystallography. In the three structures, the 5,5′-bisdiazo-dipyrromethanes form interlocked dimers through quadruple N–HN hydrogen bonds. The halogenπ synthons also provide a significant contribution to the resulting supramolecular motifs.

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Zhenming Yin
Wuyan Wang
Miao Du
Xiuguang Wang
Jianhua Guo

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Crystal engineering of 5,5′-bisdiazo-dipyrromethane with halogenπ synthons

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