In situ neutron powder diffraction and structure determination in controlled humidities

Valeska P. Ting; Paul F. Henry; Marc Schmidtmann; Chick C. Wilson; Mark T. Weller

doi:10.1039/B918702B

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Chemical Communications

Issue 48, 2009

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In situ neutron powder diffraction and structure determination in controlled humidities

Valeska P. Ting , Paul F. Henry , Marc Schmidtmann , Chick C. Wilson and Mark T. Weller

Chem. Commun., 2009, 7527-7529

DOI: 10.1039/B918702B
Received 09 Sep 2009, Accepted 20 Oct 2009
First published on the web 05 Nov 2009

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Abstract
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A controlled-humidity sample environment has been constructed, allowing bulk powder samples undergoing humidity-induced phase transitions and reactions to be studied via in situ neutron diffraction. Associated developments in data collection and analysis permit this to be achieved without the use of D₂O.

Supplementary Info

Schematic of controlled-humidity sample environment; NPD dataof zeolite LTA at 100% RH at T = 0, 100 min; table of refined atomic positions for CuSO₄ anhydrous and hydrated phases from NPD data at 298K
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Valeska P. Ting
Paul F. Henry
Marc Schmidtmann
Chick C. Wilson
Mark T. Weller

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Chemical Communications

In situ neutron powder diffraction and structure determination in controlled humidities

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