Synthesis of homogeneous antifreeze glycopeptides via a ligation–desulfurisation strategy

James Garner; Katrina A. Jolliffe; Margaret M. Harding; Richard J. Payne

doi:10.1039/B918021D

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Chemical Communications

Issue 45, 2009

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Synthesis of homogeneous antifreeze glycopeptides via a ligation–desulfurisation strategy

James Garner , Katrina A. Jolliffe , Margaret M. Harding and Richard J. Payne

Chem. Commun., 2009, 6925-6927

DOI: 10.1039/B918021D
Received 02 Sep 2009, Accepted 05 Oct 2009
First published on the web 21 Oct 2009

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Abstract
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Homogeneous glycopeptide analogues of fish antifreeze glycoproteins of discrete oligomeric length have been synthesised using a native chemical ligation–desulfurisation strategy.

Supplementary Info

Detailed procedures for the synthesis of glycopeptides andglycopeptide thioesters, and conditions for native chemicalligation and desulfurisation. Analytical data for compounds 1–10.
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Chemical Communications

Synthesis of homogeneous antifreeze glycopeptides via a ligation–desulfurisation strategy

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