A hierarchical Fe/ZSM-5 zeolite with superior catalytic performance for benzene hydroxylation to phenol

Hongchuan Xin; Arjan Koekkoek; Qihua Yang; Rutger van Santen; Can Li; Emiel J. M. Hensen

doi:10.1039/B917038C

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Chemical Communications

Issue 48, 2009

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A hierarchical Fe/ZSM-5 zeolite with superior catalytic performance for benzene hydroxylation to phenol

Hongchuan Xin , Arjan Koekkoek , Qihua Yang , Rutger van Santen , Can Li and Emiel J. M. Hensen

Chem. Commun., 2009, 7590-7592

DOI: 10.1039/B917038C
Received 18 Aug 2009, Accepted 22 Oct 2009
First published on the web 11 Nov 2009

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We report the one-step synthesis of a highly active hierarchical Fe/ZSM-5 zeolite catalyst with a strongly improved lifetime in the selective hydroxylation of benzene to phenol with nitrous oxide; compared to the best Fe/ZSM-5 catalyst, the turnover number after 24 h on stream is almost four times higher.

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Experimental details, UV-Vis, XRD, IR, SEM, active site titration, spent catalyst analysis and reaction data
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Hongchuan Xin
Arjan Koekkoek
Qihua Yang
Rutger van Santen
Can Li
Emiel J. M. Hensen

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Chemical Communications

A hierarchical Fe/ZSM-5 zeolite with superior catalytic performance for benzene hydroxylation to phenol

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